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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2385713Generated: October 29, 2026

1283095-81-7 → HCID 58203771, compound

https://huagongshe.com/reaction/2385713

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1283095-81-7HCID 41098313—
Reactant8-(1H-Pyrazol-4-yl)-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene-2-carboxylic acidHCID 58203883—
ProductHCID 58203771HCID 58203771—

Reaction Steps

Following the procedure for 103, 8-(1H-Pyrazol-4-yl)-4,5-dihydro-6-oxa-3-thia-1-aza-benzo[e]azulene-2-carboxylic acid (50.0 mg, 0.2 mmol) was reacted with (R)-N-methyl-1(tetrahydrofuran-2-yl)methanamine (1.2 equiv) to give 174 (18.4 mg, M+1 411.1)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08263633B2
Source datasetuspto-grants-2012_09
ORD IDord-38db417ff32342fe882622beba648302
Source noteuspto-grants-2012_09