HCID 11991809, compound → HCID 11991892, compound

Participants

Reaction Steps

The title compound was prepared from methyl 2-(7-phenylheptanoyl)oxazole-5-carboxylate (71 mg, 0.225 mmol) following General Procedure E. Flash chromatography (EtOAc-2% AcOH/EtOAc) yielded the title compound as a white solid (60 mg, 88%): 1H NMR (CD3OD, 600 MHz) δ 7.62 (s, 1H), 7.22-7.19 (m, 2H), 7.14-7.09 (m, 3H), 3.04 (t, 2H, J=7.5 Hz), 2.58 (t, 2H, J=7.5 Hz), 1.71-1.68 (m, 2H), 1.62-1.59 (m, 2H), 1.41-1.32 (m, 4H); 13C NMR (CD3OD, 150 MHz) δ 189.0, 159.4, 159.4, 143.3, 143.3, 134.6, 128.9, 128.7, 126.1, 39.6, 36.3, 32.0, 29.5, 29.4, 23.9; MALDI-FTMS m/z 302.1382 (M+H+, C17H20NO4, requires 302.1387).

Provenance & Evidence