HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 12397255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Hydroxypyridine-2,6-dimethanol | HCID 417366 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 12397255 | HCID 12397255 | — |
Reaction Steps
47 g (0.3 mol) of 3-hydroxy-2,6-bis(hydroxymethyl)pyridine are dissolved in 800 ml of acetonitrile. 104 g of K2CO3 (0.753 mol) and 55 ml of benzyl bromide (0.45 mol) are added. The combined mixture is brought to reflux for 12 h. After having filtered off the insoluble material, the solution is concentrated and the residue is hardened in isopropyl ether. w=39 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268810B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-6d3a61b4f8c54e54a9c8e4da800b8d85 |
| Source note | uspto-grants-2012_09 |