Thioglycolic Acid → HCID 57828149, compound

Participants

Reaction Steps

24.2 g (0.0279 mol) of 12-benzyloxy-3,6,9-tris(2-nitrobenzenesulphonyl)-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(14),11(15),12-triene are dissolved in 200 ml of DMF and then 22 g of LiOH and 21 ml of thioglycolic acid are introduced. The combined mixture is left at AT overnight. After evaporating the DMF, the residual oil is taken up in dichloromethane and the organic solution is then washed with water, dried and concentrated. A brown oil is obtained. w=15 g.

Provenance & Evidence