HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → N-[3-(2-Chloro-pyrimidin-4-yl)-benzyl]-N-pyridin-4-ylmethyl-methanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 86603252 | HCID 86603252 | — |
| Product | N-[3-(2-Chloro-pyrimidin-4-yl)-benzyl]-N-pyridin-4-ylmethyl-methanesulfonamide | HCID 86603251 | — |
Reaction Steps
Intermediate 14 was coupled with methanesulfonyl chloride following procedure D. LC-MS showed the product had the expected M+H+ of 389.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268822B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-567ad3f5c34c43c095146902761418db |
| Source note | uspto-grants-2012_09 |