HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloropyrimidine → 4-(3-Butoxy-phenyl)-2-chloro-pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloropyrimidine | HCID 77531 | — |
| Reactant | 3-Butoxyphenylboronic Acid | HCID 5084101 | — |
| Product | 4-(3-Butoxy-phenyl)-2-chloro-pyrimidine | HCID 86603273 | — |
Reaction Steps
2,4 dichloropyrimidine was coupled with 3-butoxyphenylboronic acid following procedure A. LC-MS showed the product had the expected M+H+ of 263.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268822B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-a2a20527239e4858b9cbf294012ffe52 |
| Source note | uspto-grants-2012_09 |