HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(1,1-Dimethylethyl) 2-methyl 1,2-piperazinedicarboxylate → HCID 86603316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(1,1-Dimethylethyl) 2-methyl 1,2-piperazinedicarboxylate | HCID 2756818 | — |
| Reactant | 3-(2-Chloro-pyrimidin-4-yl)-benzaldehyde | HCID 24901965 | — |
| Product | HCID 86603316 | HCID 86603316 | — |
Reaction Steps
Intermediate 1 was coupled with piperazine-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester following procedure B. LC-MS showed the product had the expected M+H+ of 447.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268822B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-3f8f6b5f0c994b64939f56d9c12e2ea0 |
| Source note | uspto-grants-2012_09 |