HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloropyrimidine → HCID 86603331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloropyrimidine | HCID 77531 | — |
| Reactant | HCID 67045047 | HCID 67045047 | — |
| Product | HCID 86603331 | HCID 86603331 | 90% |
Reaction Steps
2,4-dichloropyrimidine and (S)-tert-butyl 3-methyl-4-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenylsulfonyl)piperazine-1-carboxylate was coupled following procedure A. The yield was 90%. LC-MS showed the product was >95% pure and had the expected M+H+ of 453.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268822B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-4855dc6ca46947b781e12b24593ae4fc |
| Source note | uspto-grants-2012_09 |