HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxy-4-(methoxycarbonyl)benzeneboronic acid → HCID 66696999, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxy-4-(methoxycarbonyl)benzeneboronic acid | HCID 17750256 | — |
| Reactant | 5-[2-(4-Bromo-2-chloro-phenyl)-1-hydroxy-1-trifluoromethyl-propyl]-3-methyl-3H-benzooxazol-2-one | HCID 66696981 | — |
| Product | HCID 66696999 | HCID 66696999 | — |
Reaction Steps
The title compound was prepared in analogy to Example 117 from 5-[2-(4-bromo-2-chloro-phenyl)-1-hydroxy-1-trifluoromethyl-propyl]-3-methyl-3H-benzooxazol-2-one (obtained in Example 116, step 8) by Suzuki coupling with 3-methoxy-4-methoxycarbonylphenylboronic acid [CAS Reg. No. 603122-41-4]. MS (m/e)=550.3 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268820B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-6dee00cd53474c7693ad064be7d2e5ea |
| Source note | uspto-grants-2012_09 |