HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyano-3,5-dimethylbenzoic acid → 4-[2-(2-Chloro-4-methoxy-phenyl)-acetyl]-2,6-dimethyl-benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyano-3,5-dimethylbenzoic acid | HCID 13997879 | — |
| Reactant | 2-Chloro-4-methoxyphenylacetic acid methylester | HCID 57383507 | — |
| Product | 4-[2-(2-Chloro-4-methoxy-phenyl)-acetyl]-2,6-dimethyl-benzonitrile | HCID 66697109 | — |
Reaction Steps
The title compound was prepared in analogy to Example 138, steps 1 and 2, from (2-chloro-4-methoxy-phenyl)-acetic acid methyl ester and 4-cyano-3,5-dimethyl-benzoic acid (CAS [90924-01-0]). Orange solid. MS (m/e, ISP neg. ion)=312.1 [M−H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268820B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-f8e2e5b2a2164e98a4ceeea0ffd1115f |
| Source note | uspto-grants-2012_09 |