Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 23151266 | HCID 23151266 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 11223065 | HCID 11223065 | — |
Reaction Steps
2-ethyl-3-[4-(3-chloropropoxy)phenyl]-4(3H)-quinazolinone (19 g, 55.6 mmol), piperidine (23.7 g, 278 mmol), potassium carbonate (11.5 g, 83.4 mmol) and potassium iodide (13.8 g, 83.4 mmol) were mixed in dimethylformamide (400 mL) and stirred at 80° C. for 24 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08268842B2 |
|---|
| Source dataset | uspto-grants-2012_09 |
|---|
| ORD ID | ord-130c5c05256d4b9790a4044fdce67371 |
|---|
| Source note | uspto-grants-2012_09 |
|---|
