HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Hydroxyphenyl)boronic acid → HCID 59423920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Hydroxyphenyl)boronic acid | HCID 2773454 | — |
| Reactant | HCID 59423922 | HCID 59423922 | — |
| Product | HCID 59423920 | HCID 59423920 | — |
Reaction Steps
The title compound was prepared from the product of example 55 and 2-hydroxyphenylboronic acid, using the same method as that described for example 56. The crude compound was purified by column chromatography on silica gel, eluting with ethyl acetate followed by dichloromethane:methanol, 95:5, to afford the desired product as pale brown foam in 61% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08268881B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-1615e4c9e23b4d0dbaf55165fecdaa32 |
| Source note | uspto-grants-2012_09 |