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HRID2387794

反应详情

EQUATION

反应方程式

HRID 2387794 的结构方程式

REACTANTS

反应物

1
结构：CCCC[C@@H](CCO)Nc1nc(N)nc(C)c1C#CCNC(=O)OC(C)(C)C
HCID86633395

未命名化合物

PRODUCTS

生成物

1
结构：CCCC[C@@H](CCO)Nc1nc(N)nc(C)c1CCCNC(=O)OC(C)(C)C
HCID86633396

未命名化合物

收率 75.2%

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

The product from step (vii) (100 mg) and Pd/C (30 mg) in EtOH (5 mL) were hydrogenated under 3 bar at rt for 16 h. The catalyst was filtered off and the solvent evaporated to give the subtitle compound 76 mg.

WORKUP

后处理

  1. filtrationThe catalyst was filtered off
  2. customthe solvent evaporated