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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2387878Generated: November 3, 2026

HCID 68956100, compound → HCID 57824842, compound

https://huagongshe.com/reaction/2387878

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68956100HCID 68956100—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 57824842HCID 57824842—

Reaction Steps

The product from step (ii) (100 mg) was dissolved in EtOAc (10 mL) and Pd/C (73.9 mg) in EtOAc (1 mL) was added and the reaction stirred under hydrogen (4 bar) at rt for 16 h. The catalyst was filtered off and the solvents were evaporated. The crude product was purified by RPHPLC to give the title compound as a white solid, 22 mg.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08268990B2
Source datasetuspto-grants-2012_09
ORD IDord-e2cac6a50eac4db792b9a73d4097d357
Source noteuspto-grants-2012_09