HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hippuric Acid → HCID 86646675, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hippuric Acid | HCID 464 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 1-Ethyl-3-(3'-dimethylaminopropyl)carbodiimide | HCID 15908 | — |
| Reactant | Tert-butyl 3-aminoazetidine-1-carboxylate | HCID 1516507 | — |
| Product | HCID 86646675 | HCID 86646675 | — |
Reaction Steps
The title compound was prepared as a TFA salt from the EDCI coupling of hippuric acid (Fluka) and 3-amino-azetidine-1-carboxylic acid tert-butyl ester (BetaPharm) followed by the de-protection of N-Boc by TFA using the procedures described in Example 1, steps D and E.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08269015B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-3408af5fbf6448bebc41521359bdf618 |
| Source note | uspto-grants-2012_09 |