HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(azetidin-1-ylcarbonyl)-N-(tert-butyl)furan-2-sulfonamide → 5-(Azetidin-1-ylcarbonyl)furan-2-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(azetidin-1-ylcarbonyl)-N-(tert-butyl)furan-2-sulfonamide | HCID 39953519 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | 5-(Azetidin-1-ylcarbonyl)furan-2-sulfonamide | HCID 53628365 | — |
Reaction Steps
A solution of 5-(azetidin-1-ylcarbonyl)-N-(tert-butyl)furan-2-sulfonamide (the product of step ii) (3 g) in trifluoroacetic acid (90 mL) was stirred at room temperature. After 18 h the mixture was evaporated to dryness in vacuo. The resulting oil was triturated with Et2O and filtered to give the subtitle compound as a white solid. Yield: 1.75 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08269002B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-aaa82ae3fc2d40999e323a22e5649ed1 |
| Source note | uspto-grants-2012_09 |