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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2389167Generated: October 30, 2026

Monobenzone → 5-(6-(4-(Benzyloxy)phenoxy)naphthalen-2-yl)-2,2-dimethyl-5-nitro-1,3-dioxane

https://huagongshe.com/reaction/2389167

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMonobenzoneHCID 7638—
Reactant2,2-Dimethyl-5-nitro-5-(6-(4-phenoxyphenoxy)naphthalen-2-yl)-1,3-dioxaneHCID 86642907—
Product5-(6-(4-(Benzyloxy)phenoxy)naphthalen-2-yl)-2,2-dimethyl-5-nitro-1,3-dioxaneHCID 8664290841%

Reaction Steps

5-(6-(4-(benzyloxy)phenoxy)naphthalen-2-yl)-2,2-dimethyl-5-nitro-1,3-dioxane was synthesized as per 2,2-dimethyl-5-nitro-5-(6-(4-phenoxyphenoxy)naphthalen-2-yl)-1,3-dioxane (Example 243) in 41% yield using 4-(benzyloxy)phenol as the reagent.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08269043B2
Source datasetuspto-grants-2012_09
ORD IDord-a72647ec771a4b8faa7f5d659ec88c77
Source noteuspto-grants-2012_09