Geranylamine → HCID 59266735, compound

HRID 2389219Notes

Reaction equation

HRID 2389219 reaction equation
[CH2:1]([NH2:11])/[CH:2]=[C:3](/[CH2:5][CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])\[CH3:4].[Cl-].[CH2:13]([O:15][C:16](=[O:20])[C:17](O)=[O:18])[CH3:14]>>[CH2:13]([O:15][C:16](=[O:20])[C:17]([NH:11][CH2:1]/[CH:2]=[C:3](\[CH3:4])/[CH2:5][CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])=[O:18])[CH3:14]

Participants

3

Reactant 2

HCID 5475462GeranylamineHCID 23618337Oxalic acid monoethylester chloride

Product 1

HCID 59266735HCID 59266735, compound

Procedure

Said substance is manufactured according to AAV 1, by converting geranylamine and oxalic acid monoethylester chloride with each other and the product is purified by column chromatography (pentane/diethyl ether=2/1).

Workup

  1. customis purified by column chromatography (pentane/diethyl ether=2/1)

Sources & evidence

ORD record
ord-c8cc00800de84193aefcc7a4e1298fef
Source dataset
uspto-grants-2012_09
Patent number
US08273398B2

Reaction notes

Loading…