Geranylamine → HCID 59266740, compound

HRID 2389220Notes

Reaction equation

HRID 2389220 reaction equation
[CH2:1]([NH2:11])/[CH:2]=[C:3](/[CH2:5][CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])\[CH3:4].[Cl-].[CH3:13][O:14][C:15](=[O:19])[C:16](O)=[O:17]>>[CH3:13][O:14][C:15](=[O:19])[C:16]([NH:11][CH2:1]/[CH:2]=[C:3](\[CH3:4])/[CH2:5][CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])=[O:17]

Participants

3

Reactant 2

HCID 5475462GeranylamineHCID 86640482Oxalic acid monomethyl ester chloride

Product 1

HCID 59266740HCID 59266740, compound

Procedure

Said substance is manufactured according to AAV 1, by converting geranylamine and oxalic acid monomethylester chloride with each other and the product is purified by column chromatography (pentane/diethyl ether=1/1).

Workup

  1. customis purified by column chromatography (pentane/diethyl ether=1/1)

Sources & evidence

ORD record
ord-d718f6d591384f22956d8f5d34237a01
Source dataset
uspto-grants-2012_09
Patent number
US08273398B2

Reaction notes

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