HCID 5362850, compound → HCID 59266734, compound

HRID 2389221Notes

Reaction equation

HRID 2389221 reaction equation
[CH2:1]([NH2:11])/[CH:2]=[C:3](\[CH2:5][CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])/[CH3:4].[Cl-].[CH3:13][O:14][C:15](=[O:19])[C:16](O)=[O:17]>>[CH3:13][O:14][C:15](=[O:19])[C:16]([NH:11][CH2:1]/[CH:2]=[C:3](/[CH3:4])\[CH2:5][CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])=[O:17]

Participants

3

Reactant 2

HCID 5362850HCID 5362850, compoundHCID 86640482Oxalic acid monomethyl ester chloride

Product 1

HCID 59266734HCID 59266734, compound

Procedure

Said substance is manufactured according to AAV 1, by converting nerylamine and oxalic acid monomethylester chloride with each other and the product is purified by column chromatography (pentane/diethyl ether=3/2).

Workup

  1. customis purified by column chromatography (pentane/diethyl ether=3/2)

Sources & evidence

ORD record
ord-66588540920b44d897fa8bcdc819c849
Source dataset
uspto-grants-2012_09
Patent number
US08273398B2

Reaction notes

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