HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → HCID 59826488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 12273165 | HCID 12273165 | — |
| Product | HCID 59826488 | HCID 59826488 | 60% |
Reaction Steps
Procedure B was performed with 2-bromo-2′chloro-5′-nitroacetophenone (14.16 g, 50 mmol), 1,2-phenylenediamine (13.1 g, 120 mmol) and NaOAc (12.4, 150 mmol) to give the desired 2-(2-chloro-5-nitro-phenyl)-quinoxaline (8.6 g, 30 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273743B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-aff46498e2d443828ddfbb45958e4838 |
| Source note | uspto-grants-2012_09 |