3-Chlorothiophenol → HCID 58022625, compound
Reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([SH:8])[CH:5]=[CH:6][CH:7]=1.[Cl:9][C:10]1[CH:17]=[C:16](F)[CH:15]=[CH:14][C:11]=1[CH:12]=[O:13]>>[Cl:9][C:10]1[CH:17]=[C:16]([S:8][C:4]2[CH:5]=[CH:6][CH:7]=[C:2]([Cl:1])[CH:3]=2)[CH:15]=[CH:14][C:11]=1[CH:12]=[O:13]Participants
3
Procedure
3-Chlorobenzenethiol and 2-chloro-4-fluorobenzaldehyde were reacted according to the same experiment procedures as in Reference Example 1 of the pamphlet of WO 03029205 to obtain the target product as a colorless oil.
Sources & evidence
- ORD record
- ord-b7fe821d7a244fb6b0f706d3ea6d2a38
- Source dataset
- uspto-grants-2012_09
- Patent number
- US08273748B2
Reaction notes
Loading…