2-Chloro-4-fluorobenzaldehyde → HCID 58022610, compound
Reaction equation
[CH2:1]([C:3]1[CH:4]=[C:5]([SH:9])[CH:6]=[CH:7][CH:8]=1)[CH3:2].[Cl:10][C:11]1[CH:18]=[C:17](F)[CH:16]=[CH:15][C:12]=1[CH:13]=[O:14]>>[Cl:10][C:11]1[CH:18]=[C:17]([S:9][C:5]2[CH:6]=[CH:7][CH:8]=[C:3]([CH2:1][CH3:2])[CH:4]=2)[CH:16]=[CH:15][C:12]=1[CH:13]=[O:14]Participants
3
Procedure
3-Ethylbenzenethiol and 2-chloro-4-fluorobenzaldehyde were reacted according to the same experiment procedures as in Reference Example 1 of the pamphlet of WO 03029205 to obtain the target product as a colorless oil.
Sources & evidence
- ORD record
- ord-a550299e4afe451ab8fe0eddc8451d73
- Source dataset
- uspto-grants-2012_09
- Patent number
- US08273748B2
Reaction notes
Loading…