反应详情

tert-Butyl carbamate 116 (75 mg, 0.12 mmol) is deprotected using Method E. On removal of the solvent in vacuo, the residue obtained is dissolved in water (5 mL) and washed with TBME (3×5 mL). Reduction of the aqueous phase in vacuo affords the title product.

1. customOn removal of the solvent in vacuo
2. customthe residue obtained
3. washwashed with TBME (3×5 mL)