HCID 59312932, compound → HCID 86641363, compound

HRID 2389827Notes

Reaction equation

HRID 2389827 reaction equation
Cl[C:2]1[N:7]2[CH:8]=[CH:9][N:10]=[C:6]2[CH:5]=[C:4]([C:11]2[CH:16]=[CH:15][C:14]([Cl:17])=[CH:13][C:12]=2[Cl:18])[N:3]=1.[CH:19]([OH:21])=[O:20].[NH2:22][CH2:23][CH2:24][N:25]([CH3:36])[C:26]1[N:31]=[C:30]([NH2:32])[C:29]([N+:33]([O-:35])=[O:34])=[CH:28][CH:27]=1>>[CH:19]([OH:21])=[O:20].[Cl:18][C:12]1[CH:13]=[C:14]([Cl:17])[CH:15]=[CH:16][C:11]=1[C:4]1[N:3]=[C:2]([NH:22][CH2:23][CH2:24][N:25]([CH3:36])[C:26]2[N:31]=[C:30]([NH2:32])[C:29]([N+:33]([O-:35])=[O:34])=[CH:28][CH:27]=2)[N:7]2[CH:8]=[CH:9][N:10]=[C:6]2[CH:5]=1

Participants

3

Reactant 2

HCID 59312932HCID 59312932, compoundHCID 86641364HCID 86641364, compound

Product 1

HCID 86641363HCID 86641363, compound

Procedure

In analogy to the procedure for preparing Example 5, the product is obtained by reacting 5-chloro-7-(2,4-dichlorophenyl)imidazo[1,2-c]pyrimidine (Example 6A) with N6-(2-aminoethyl)-N6-methyl-3-nitropyridine-2,6-diamine formate (preparation analogous to Example 14A).

Workup

  1. customIn analogy to the procedure for preparing Example 5
  2. customthe product is obtained

Sources & evidence

ORD record
ord-d38bcc6d3aae4c9ca4908eb71ab7280b
Source dataset
uspto-grants-2012_09
Patent number
US08273752B2

Reaction notes

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