HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2389928Generated: October 26, 2026
Diethyl Ether → 5-Amino-2-methylfuro[3,2-c]pyridin-5-ium 2,4-dinitrobenzenolate
https://huagongshe.com/reaction/2389928
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | O-(2,4-dinitrophenyl)hydroxylamine | HCID 87140 | — |
| Reactant | 2-Methylfuro[3,2-c]pyridine | HCID 13803064 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 5-Amino-2-methylfuro[3,2-c]pyridin-5-ium 2,4-dinitrobenzenolate | HCID 86638667 | 82% |
Reaction Steps
A mixture of 2-methylfuro[3,2-c]pyridine (1.20 g, 8.99 mmol) and 1-(aminooxy)-2,4-dinitrobenzene (1.79 g, 8.99 mmol) in acetonitrile (9.0 mL) was stirred at 30° C. for 22 hr, and diethyl ether was added. The resulting precipitate was collected by filtration to give the title compound (2.44 g, yield 82%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08273761B2 |
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| Source dataset | uspto-grants-2012_09 |
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| ORD ID | ord-5efe2aa9b11b427e9e818c27dcb2339a |
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| Source note | uspto-grants-2012_09 |
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