Formaldehyde → HCID 59323360, compound

HRID 2390027Notes

Reaction equation

HRID 2390027 reaction equation
[CH2:1]([NH:8][CH2:9][CH2:10][N:11]1[CH:20]([CH2:21][C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[CH2:19][C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[CH2:12]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:28]=O>>[CH2:1]([N:8]([CH3:28])[CH2:9][CH2:10][N:11]1[CH:20]([CH2:21][C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[CH2:19][C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[CH2:12]1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 712FormaldehydeHCID 59323388HCID 59323388, compound

Product 1

HCID 59323360HCID 59323360, compound

Procedure

The reaction and treatment were carried out in the same manner as in Example 1-g) using N-benzyl-2-[3-benzyl-3,4-dihydroisoquinolin-2(1H)-yl]ethanamine obtained in Example 1 as a starting material and using paraformaldehyde to obtain a title compound as a pale yellow oily substance.

Workup

  1. customThe reaction and treatment

Sources & evidence

ORD record
ord-552ef79622204d91935dfbe635f9ecf6
Source dataset
uspto-grants-2012_09
Patent number
US08273766B2

Reaction notes

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