HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl(4-chloro-2-ethynylphenoxy)acetate → Tert-butyl(4-cyano-2-ethynylphenoxy)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl(4-chloro-2-ethynylphenoxy)acetate | HCID 56594381 | — |
| Reactant | Tert-butyl{4-cyano-2-[(trimethylsilyl)ethynyl]phenoxy}acetate | HCID 58521908 | — |
| Product | Tert-butyl(4-cyano-2-ethynylphenoxy)acetate | HCID 58522073 | 72% |
Reaction Steps
Following the general method as outlined in Intermediate 3, starting from tert-butyl{4-cyano-2-[(trimethylsilyl)ethynyl]phenoxy}acetate (Intermediate 45), the title compound was obtained as an oil in 72% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-5865ed61d9e3490ea8438efdd672659c |
| Source note | uspto-grants-2012_09 |