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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2390175Generated: October 30, 2026

1-Isopropenyl-4-(methylsulfonyl)-2-nitrobenzene → 2-Isopropenyl-5-(methylsulfonyl)aniline

https://huagongshe.com/reaction/2390175

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Isopropenyl-4-(methylsulfonyl)-2-nitrobenzeneHCID 58521898—
Reactant5-(methylsulfonyl)-2-[(1E)-prop-1-en-1-yl]anilineHCID 58522013—
Product2-Isopropenyl-5-(methylsulfonyl)anilineHCID 58521961—

Reaction Steps

Following the general method as outlined in Intermediate 60, starting from 1-isopropenyl-4-(methylsulfonyl)-2-nitrobenzene (Intermediate 88), the title compound was obtained as an orange solid after purification by flash column chromatography (silica), eluting with cyclohexane containing increasing amounts of EtOAc.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08273769B2
Source datasetuspto-grants-2012_09
ORD IDord-00bb0b92201f457db68e0d6db14409a9
Source noteuspto-grants-2012_09