HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-5-methylsulfonylnitrobenzene → 4-(Methylsulfonyl)-2-nitro-1-vinylbenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-5-methylsulfonylnitrobenzene | HCID 2060366 | — |
| Reactant | 2-Ethenyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane | HCID 5233012 | — |
| Product | 4-(Methylsulfonyl)-2-nitro-1-vinylbenzene | HCID 58521924 | — |
Reaction Steps
Following the general method as outlined in Intermediate 20, starting from 2-bromo-5-methylsulfonylnitrobenzene and vinylboronic acid pinacol ester, the title compound was obtained as a brown oil in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-c5ca50a4fa81470985545ba9d3a26aac |
| Source note | uspto-grants-2012_09 |