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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2390227Generated: November 1, 2026

Tert-butyl(4-chloro-2-ethynylphenoxy)acetate → HCID 58521923, compound

https://huagongshe.com/reaction/2390227

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTert-butyl(4-chloro-2-ethynylphenoxy)acetateHCID 56594381—
ReactantHCID 58521895HCID 58521895—
ProductHCID 58521923HCID 58521923—

Reaction Steps

Following the general method as outlined in Intermediate 20, starting from (4-chloro-2-ethynyl-phenoxy)-acetic acid tert-butyl ester (Intermediate 3) and 3-bromo-N-(3-dimethylamino-propyl)-4,N-dimethyl-benzenesulfonamide (Intermediate 151), the title compound was obtained after purification by preparative HPLC.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08273769B2
Source datasetuspto-grants-2012_09
ORD IDord-79aef51dd02e421c88807e0c948f8d64
Source noteuspto-grants-2012_09