HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Methoxyphenyl)boronic acid → HCID 58522028, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Methoxyphenyl)boronic acid | HCID 201262 | — |
| Reactant | HCID 58521957 | HCID 58521957 | — |
| Reactant | HCID 58521981 | HCID 58521981 | — |
| Product | HCID 58522028 | HCID 58522028 | 73% |
Reaction Steps
Following the general method as outlined in Intermediate 203, starting from 4-bromo-1-iodo-2-(methylsulfonyl)benzene (Intermediate 202) and 4-methoxyphenylboronic acid, the title compound was obtained as a brown solid in 73% yield after purification by flash column chromatography (silica), eluting with cyclohexane containing increasing amounts of EtOAc.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-823ecb71ca7544ab88307ef26f30bf09 |
| Source note | uspto-grants-2012_09 |