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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2390264Generated: October 31, 2026

(3-Methoxyphenyl)boronic acid → HCID 58522076, compound

https://huagongshe.com/reaction/2390264

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(3-Methoxyphenyl)boronic acidHCID 2734370—
ReactantHCID 58521957HCID 58521957—
ReactantHCID 58521981HCID 58521981—
ProductHCID 58522076HCID 5852207674%

Reaction Steps

Following the general method as outlined in Intermediate 203, starting from 4-bromo-1-iodo-2-(methylsulfonyl)benzene (Intermediate 202) and 3-methoxyphenylboronic acid, the title compound was obtained as a brown sticky solid in 74% yield after purification by flash column chromatography (silica), eluting with cyclohexane containing increasing amounts of EtOAc.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08273769B2
Source datasetuspto-grants-2012_09
ORD IDord-7a9a0c335c3c44cab3a10adad1e0c747
Source noteuspto-grants-2012_09