HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 91455044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 58522032 | HCID 58522032 | — |
| Product | HCID 91455044 | HCID 91455044 | — |
Reaction Steps
Following the general method as outlined in Intermediate 223, starting from tert-butyl{2-[(4-aminophenyl)ethynyl]-4-chlorophenoxy}acetate (Intermediate 222) and benzoyl chloride, the title compound was obtained after purification by flash column chromatography (silica), eluting with cyclohexane containing increasing amounts of EtOAc.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-69230b90a289458395de1882245ad90d |
| Source note | uspto-grants-2012_09 |