HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl(4-chloro-2-ethynylphenoxy)acetate → {4-Chloro-2-[(4-hexylpyridin-3-yl)ethynyl]phenoxy}acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl(4-chloro-2-ethynylphenoxy)acetate | HCID 56594381 | — |
| Reactant | 3-Bromo-4-hexylpyridine | HCID 58521884 | — |
| Product | {4-Chloro-2-[(4-hexylpyridin-3-yl)ethynyl]phenoxy}acetic acid | HCID 56594513 | — |
Reaction Steps
Following the general method as outlined in Example 8, starting from tert-butyl(4-chloro-2-ethynylphenoxy)acetate (Intermediate 3) and 3-bromo-4-hexylpyridine (Intermediate 13), the title compound was obtained as a beige solid after purification by preparative HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-0896e4b5527b469eb69e4ed1da398c6a |
| Source note | uspto-grants-2012_09 |