HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-5-(methylsulfonyl)pyridine → HCID 56595046, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-5-(methylsulfonyl)pyridine | HCID 22391981 | — |
| Reactant | Tert-butyl(4-chloro-2-ethynylphenoxy)acetate | HCID 56594381 | — |
| Product | HCID 56595046 | HCID 56595046 | — |
Reaction Steps
Following the general method as outlined in Example 35, starting from tert-butyl(4-chloro-2-ethynyl phenoxy)acetate (Intermediate 3) and 5-bromo-3-methylsulfonylpyridine (Combiblocks), the title compound was obtained as a white solid after purification by flash column chromatography (silica).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-e951ebb490a7403699e7c36254a3b2d8 |
| Source note | uspto-grants-2012_09 |