HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 7123352, compound → HCID 20635627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 7123352 | HCID 7123352 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 20635627 | HCID 20635627 | 87.6% |
Reaction Steps
A mixture of 2.48 g of N-propyl-2-nitro-4-trifluoromethylaniline, 30 ml of ethyl acetate and 5% palladium charcoal was stirred for 1.5 hours at room temperature under a hydrogen atmosphere of about 1 atm. The reaction mixture was filtrated through Celite (registered trademark). The filtrate was washed with water, dried over sodium sulfate, then, concentrated under reduced pressure, to obtain 1.91 g of N1-propyl-4-trifluoromethylbenzene-1,2-diamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273764B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-0af0e73c112c4572950936a4b80b4b45 |
| Source note | uspto-grants-2012_09 |