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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2390494Generated: November 1, 2026

HCID 7123352, compound → HCID 20635627, compound

https://huagongshe.com/reaction/2390494

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 7123352HCID 7123352—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 20635627HCID 2063562787.6%

Reaction Steps

A mixture of 2.48 g of N-propyl-2-nitro-4-trifluoromethylaniline, 30 ml of ethyl acetate and 5% palladium charcoal was stirred for 1.5 hours at room temperature under a hydrogen atmosphere of about 1 atm. The reaction mixture was filtrated through Celite (registered trademark). The filtrate was washed with water, dried over sodium sulfate, then, concentrated under reduced pressure, to obtain 1.91 g of N1-propyl-4-trifluoromethylbenzene-1,2-diamine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08273764B2
Source datasetuspto-grants-2012_09
ORD IDord-0af0e73c112c4572950936a4b80b4b45
Source noteuspto-grants-2012_09