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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2390719Generated: October 29, 2026

Diethylamine → HCID 18451156, compound

https://huagongshe.com/reaction/2390719

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethylamineHCID 8021—
ReactantN-{4-[4-amino-7-(3-formylphenyl)thieno[3,2-c]pyridin-3-yl]-2-methoxyphenyl}-1-methyl-1H-indole-2-carboxamideHCID 18451194—
ProductHCID 18451156HCID 18451156—

Reaction Steps

The title compound was prepared using N-{4-[4-amino-7-(3-formylphenyl)thieno[3,2-c]pyridin-3-yl]-2-methoxyphenyl}-1-methyl-1H-indole-2-carboxamide, N,N-diethylamine, and General Procedure B. 1H NMR (DMSO-d6, 400 MHz) δ 9.53 (s, 1H), 8.02 (d, 1H), 7.92 (s, 1H), 7.71 (d, 1H), 7.67 (s, 1H), 7.64 (m, 2H), 7.60 (s, 1H), 7.52 (m, 1H), 7.47 (t, 1H), 7.35 (m, 1H), 7.32 (m, 1H), 7.24 (m, 1H), 7.15 (m, 1H), 7.12 (m, 1H), 5.62 (br, 2H), 4.05 (s, 3H), 3.92 (s, 3H), 3.62 (s, 2H), 2.53 (qt, 4H), 1.02 (t, 6H); MS: (MH)+ 590.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08273736B2
Source datasetuspto-grants-2012_09
ORD IDord-7f0e8489c53945c9a929b9511dc11e95
Source noteuspto-grants-2012_09