HRID2390955
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution of 3-(acetoxyimino)pentane-2,4-dione 12 (0.2 mmol, 1.0 eq) and (E)-hex-2-enal (0.5 mmol, 2.5 eq) in toluene (0.8 mL) was added catalyst VII (0.04 mmol, 0.2 eq) in toluene (0.2 mL) at room temperature. The resulting mixture was stirred vigorously. After 12 hours the reaction still didn't proceed.
WORKUP
后处理
- customAfter 12 hours the reaction