HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 1-([1,1'-biphenyl]-4-yl)cyclopropanecarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 1-(4-Biphenylyl)cyclopropanecarboxylic acid | HCID 21552263 | — |
| Product | Ethyl 1-([1,1'-biphenyl]-4-yl)cyclopropanecarboxylate | HCID 66660499 | — |
Reaction Steps
1-(Biphenyl-4-yl)cyclopropanecarboxylic acid (10 g, 42 mmol), ethanol (100 mL) and sulfuric acid (40 mL) were heated to 65° C. for 4 hours. The product was extracted with CH2Cl2 and water (2×), dried and evaporated to yield 9.5 g of 1-(biphenyl-4-yl)cyclopropanecarboxylic acid ethyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273780B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-799699c7a67a44c3aa8d7346f21d0532 |
| Source note | uspto-grants-2012_09 |