HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1-(4-Bromophenyl)cyclopropane-1-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 1-(4-Bromophenyl)Cyclopropanecarbonitrile | HCID 2795273 | — |
| Solvent | Ethylene Glycol | HCID 174 | — |
| Product | 1-(4-Bromophenyl)cyclopropane-1-carboxylic acid | HCID 16227966 | — |
Reaction Conditions
| Temperature | 180 °C |
|---|
Reaction Steps
1-(4-Bromo-phenyl)-cyclopropanecarbonitrile (5 g, 22.5 mmol) and potassium hydroxide (5 g, 89.3 mmol) were combined in ethylene glycol (70 mL), and the reaction was stirred at 180° C. for 4 hours. The mixture was poured into H2O, acidified, and filtered to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273780B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-3480db001dbb49009a96b002ee53cc71 |
| Source note | uspto-grants-2012_09 |