HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 66660384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 1-(3-{[tert-Butyl(dimethyl)silyl]oxy}phenyl)ethan-1-one | HCID 14361489 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66660384 | HCID 66660384 | — |
Reaction Steps
1-[3-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-ethanone (3.67 mmol) in MeOH (5 mL) was treated with sodium borohydride (0.139 g, 3.67 mmol). The reaction was stirred for 20 minutes, and then standard work-up provided the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273780B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-1b1d443c62824880a8482722e262b7f3 |
| Source note | uspto-grants-2012_09 |