1-Phenylethanol → HCID 57383266, compound

HRID 2391110Notes

Reaction equation

[CH3:1][C:2]1[C:6]([NH:7][C:8]([O:10][C@@H:11]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH3:12])=[O:9])=[C:5]([C:19]2[CH:24]=[CH:23][C:22]([C:25]3[CH:30]=[CH:29][C:28]([C:31]4([C:34]([OH:36])=[O:35])[CH2:33][CH2:32]4)=[CH:27][CH:26]=3)=[CH:21][CH:20]=2)[O:4][N:3]=1.C1(C(O)C)C=CC=CC=1>>[CH3:1][C:2]1[C:6]([NH:7][C:8]([O:10][CH:11]([C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=2)[CH3:12])=[O:9])=[C:5]([C:19]2[CH:24]=[CH:23][C:22]([C:25]3[CH:26]=[CH:27][C:28]([C:31]4([C:34]([OH:36])=[O:35])[CH2:33][CH2:32]4)=[CH:29][CH:30]=3)=[CH:21][CH:20]=2)[O:4][N:3]=1

Participants

Reactant 2

HCID 74091-Phenylethanol

HCID 49792850BMS-986020

Product 1

HCID 57383266HCID 57383266, compound

Procedure

Prepared according to the procedure described in Example 1 for Compound 1 but using racemic 1-phenylethyl alcohol in place of (R)-(+)-1-phenylethyl alcohol.

Workup

customPrepared

Sources & evidence

ORD record: ord-718a442aa8b34f6db0b808e3f1276849
Source dataset: uspto-grants-2012_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08273780B2

Reaction notes

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