Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2391152Generated: October 30, 2026

1,5-Dibromopentane → HCID 57441040, compound

https://huagongshe.com/reaction/2391152

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,5-DibromopentaneHCID 8100—
ReactantSodium hydrideHCID 24758—
ReactantMethyl 3-(cyanomethyl)benzoateHCID 10821136—
SolventDimethyl SulfoxideHCID 679—
ProductHCID 57441040HCID 5744104068%

Reaction Steps

Using methyl 3-(cyanomethyl)benzoate (1.5 g, 8.6 mmol), sodium hydride (60% in oil, 1.0 g, 26 mmol), 1,5-dibromopentane (3.0 g, 13 mmol) and dimethyl sulfoxide (30 mL) as starting materials and in the same manner as in Reference Example 31, the title compound (1.4 g, 68%) was obtained as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08273741B2
Source datasetuspto-grants-2012_09
ORD IDord-1022b5be64174b4aa53402e383e7ff2c
Source noteuspto-grants-2012_09