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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2391279Generated: October 30, 2026

Hydroxybenzenesulfonic acid → HCID 86630643, compound

https://huagongshe.com/reaction/2391279

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxybenzenesulfonic acidHCID 15619088—
ReactantTak-593HCID 24767976—
SolventEthanolHCID 702—
ProductHCID 86630643HCID 8663064375%

Reaction Steps

Using N-[5-({2-[(cyclopropylcarbonyl)amino]imidazo[1,2-b]pyridazin-6-yl}oxy)-2-methylphenyl]-1,3-dimethyl-1H-pyrazole-5-carboxamide (2.00 g, 4.49 mmol), ethanol (100 mL) and benzenesulfonic acid monohydrate (0.83 g, 4.71 mmol), and in the same manner as in Example 152, the title compound (2.02 g, 75%) was obtained as white crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08273741B2
Source datasetuspto-grants-2012_09
ORD IDord-802f911a50ec42f6b4655f947a532012
Source noteuspto-grants-2012_09