HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thioacetamide → HCID 86686502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thioacetamide | HCID 2723949 | — |
| Reactant | HCID 86686500 | HCID 86686500 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86686502 | HCID 86686502 | 92.5% |
Reaction Steps
18.5 g 5-bromo-6-methylazepan-4-one hydrobromic acid salt and 5.0 g thioacetamide were dissolved in 125 mL ethanol. The mixture was heated for 3 h under reflux. The solids were removed by filtration and the filtrate was concentrated in vacuo. 100 mL acetonitrile was added and the precipitate formed was isolated by filtration to yield 15.7 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642774B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-fb49b11113e8489daf7fc6157f06fa68 |
| Source note | uspto-grants-2014_02 |