HRID239151

反应详情

EQUATION

反应方程式

HRID 239151 的结构方程式

REACTANTS

反应物

2

结构：O=S(Cl)Cl

Thionyl chloride

Cl2OS

结构：Cc1cc(C(=O)O)ccc1F

4-Fluoro-3-methylbenzoic acid

C8H7FO2

PRODUCTS

生成物

1

结构：Cc1cc(C(=O)Cl)ccc1F

4-Fluoro-3-methylbenzoyl chloride

C8H6ClFO

收率 100%

PROCEDURE

实验过程

10 g 4-fluoro-3-methyl-benzoic acid in 150 g thionylchloride was refluxed 1 h. The reaction was evaporated to give 11.2 g desired product.

WORKUP

后处理

customThe reaction was evaporated