HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 25113648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 86647101 | HCID 86647101 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 25113648 | HCID 25113648 | — |
Reaction Steps
In a similar manner as described for example 6, 58 mg of [1-(5-carbamoyl-4-{[2-(trifluoromethyl)benzyl]oxy}-2-thienyl)-1H-imidazo[4,5-c]pyridin-6-yl]methyl methanesulfonate (compound A1) and 200 mg of 1-methylpiperazine in 5 ml dichloromethane yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273890B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-8576ec06690243e9842e3b06d85bb8b4 |
| Source note | uspto-grants-2012_09 |