HCID 52915464, compound → Benzyl 2,3,6,7-tetrahydro-1H-azepine-1-carboxylate

Participants

Reaction Conditions

Reaction Steps

0.15 g Grubb's 2 catalyst was added to a solution of 8 g benzyl dibut-3-enylcarbamate in 680 mL toluene and heated at 50° C. for 5 h. The solvent was removed and the residue was purified by chromatographie on silica gel (ethyl acetate/hexane 1:5) to yield 6.6 g of the desired product. (M+H)+: 232

Provenance & Evidence