Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2391820Generated: October 30, 2026

3-Aminopyridine → HCID 59292880, compound

https://huagongshe.com/reaction/2391820

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-AminopyridineHCID 10009—
ReactantHCID 59292875HCID 59292875—
SolventDichloromethane methanolHCID 21226129—
ProductHCID 59292880HCID 59292880—

Reaction Steps

The title compound was prepared in analogy to the procedure described in Step 14.1 but using 3-aminopyridine, 8-(2,6-dichloro-3,5-dimethoxy-phenyl)-2-(4-ethyl-piperazin-1-ylmethyl)-quinoxaline-5-carboxylic acid (Step 83.1) and stirring the reaction mixture for 2 days at rt. Title compound: ESI-MS: 581.0/583.2 [M+H]+; tR=3.04 min (System 1); TLC: Rf=0.33 (DCM/MeOH, 9:1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08273882B2
Source datasetuspto-grants-2012_09
ORD IDord-64bdfa70f9bd4840b66c1c3c203ab543
Source noteuspto-grants-2012_09