HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminopyridine → HCID 59292880, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminopyridine | HCID 10009 | — |
| Reactant | HCID 59292875 | HCID 59292875 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 59292880 | HCID 59292880 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described in Step 14.1 but using 3-aminopyridine, 8-(2,6-dichloro-3,5-dimethoxy-phenyl)-2-(4-ethyl-piperazin-1-ylmethyl)-quinoxaline-5-carboxylic acid (Step 83.1) and stirring the reaction mixture for 2 days at rt. Title compound: ESI-MS: 581.0/583.2 [M+H]+; tR=3.04 min (System 1); TLC: Rf=0.33 (DCM/MeOH, 9:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273882B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-64bdfa70f9bd4840b66c1c3c203ab543 |
| Source note | uspto-grants-2012_09 |